Optimization of anethole determination using differential pulse voltammetry on glassy carbon electrode, boron doped diamond electrode and carbon paste electrode

Autor

  • Szymon Wójcik Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie
  • Małgorzata Jakubowska Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie

DOI:

https://doi.org/10.5604/01.3001.0012.8152

Słowa kluczowe:

anethole, voltammetry

Abstrakt

Voltammetry is the general term for all techniques in which the current is measured as a function of electrode potential. The voltammetric techniques can be applied for the quantitative analysis of inorganic and organic species and are best suited for substances which can be either oxidized or reduced on electrodes. These techniques are characterized by high sensitivity which results in the possibility of performing determinations at a low concentration level. In voltammetry, many different types of working electrodes are applied. One of the important groups are solid electrodes, among which carbon electrodes play an important role. They represent a good alternative to mercury electrodes, however, surface preparation before the usage is required. In this work anethole determination will be presented using three types of carbon electrodes: glassy carbon electrode, boron doped diamond electrode and carbon paste electrode. Optimization process will be also described.

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Comparison of anethole voltammograms in optimal measurement conditions after background correction, successive additions of the anethole standard from 2 μl to 10 μl, every 2 μl, green voltammograms correspond to the GC electrode, blue voltammograms correspond to the CP electrode

Opublikowane

2018-12-27

Jak cytować

Wójcik, S., & Jakubowska, M. (2018). Optimization of anethole determination using differential pulse voltammetry on glassy carbon electrode, boron doped diamond electrode and carbon paste electrode. Science, Technology and Innovation, 3(2), 21–26. https://doi.org/10.5604/01.3001.0012.8152

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